Nanoplates of h-WO3: synthesis, micromorphology, characterization

I.B. Troitskaia, T.A. Gavrilova show affiliations and emails
Received: 03 March 2011; Revised: 16 March 2011; Accepted: 24 March 2011
This paper is written in Russian
Citation: I.B. Troitskaia, T.A. Gavrilova. Nanoplates of h-WO3: synthesis, micromorphology, characterization. Lett. Mater., 2011, 1(1) 65-69
BibTex   https://doi.org/ 10.22226/2410-3535-2011-1-65-69

Abstract

Nanoplates of h-WO3 (P6/mmm, PDF 33-1387) with ~10 nm thickness, up to 200 nm diameter and pale yellow color have been precipitated from aqua ammonium tungstate solution with nitric acid. The h - β phase transition at T = 385oC has been established with DSC together with XRD. IR and Raman spectra are recorded both for precipitated and calcined phases.

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