Nanoplates of h-WO3: synthesis, micromorphology, characterization

I.B. Troitskaia1, T.A. Gavrilova1
1Institute of Semiconductor Physics, SB RAS, Lavrentieva Ave, 13, 630090 Novosibirsk
Abstract
Nanoplates of h-WO3 (P6/mmm, PDF 33-1387) with ~10 nm thickness, up to 200 nm diameter and pale yellow color have been precipitated from aqua ammonium tungstate solution with nitric acid. The h - β phase transition at T = 385oC has been established with DSC together with XRD. IR and Raman spectra are recorded both for precipitated and calcined phases.
Received: 03 March 2011   Revised: 16 March 2011   Accepted: 24 March 2011
Views: 67   Downloads: 9
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