Structure and mechanical behavior of aluminum alloy 1570C processed by multidirectional forging with decreasing temperature

O.E. Latypova, O.S. Sitdikov, E.V. Avtokratova, M.V. Markushev показать трудоустройства и электронную почту
Получена 08 июля 2026; Принята 19 августа 2026;
Эта работа написана на английском языке
Цитирование: O.E. Latypova, O.S. Sitdikov, E.V. Avtokratova, M.V. Markushev. Structure and mechanical behavior of aluminum alloy 1570C processed by multidirectional forging with decreasing temperature. Письма о материалах. 2026. Т.16. №3. С.291-299
BibTex   https://doi.org/10.48612/letters/2026-3-291-299

Аннотация

Two step MF (325 → 250°C) of alloy 1570C uniquely combines grain refinement (~1.5 μm), increased strength (YS +25 MPa), and high strain rate SP at 400°C (~1000% at >10⁻¹ s⁻¹), but with reduced thermal stability (abnormal grain growth onset at 425°C vs. >450°C after first step at 325°C). Forging at 250°C is the critical lower limit for safe deformation without β phase precipitation and reveals the dual role of enhanced stored dislocation density: beneficial for SP at 350–400°C, but detrimental at ≥450°C via abnormal grain growthThe effect of two-step isothermal multidirectional forging (MF) with decreasing temperature (325 → 250°C) on the structural and mechanical behavior of aluminum alloy 1570C (Al-5Mg-0.2Sc-0.08Zr) was studied. The first-step temperature (325°C) was chosen due to the optimal balance between dynamic recrystallization and grain growth, while the second one (250°C) was limited by the solvus temperature of the brittle β-phase (Al3Mg2) to avoid its undesirable precipitation and embrittlement. The first MF step produced an ultrafine-grained structure (≈2.0 μm, 78 % HABs). Subsequent deformation at 250°C refined the structure to ≈1.5 μm, increased strength (YS + 25 MPa, UTS +15 MPa, HV +10) with approximately 33 % elongation, and no β-phase was detected; however, thermal stability was reduced, with the onset of abnormal grain growth shifting from >450°C to 425°C. The two-step processed material exhibits dual superplastic behavior: at ≥450°C, superplastic performance deteriorates and elongation is limited to ≈1700 % (vs. 2800 % after 325°C forging); however, at around 400°C, high-strain-rate superplasticity (≈1000 % at up to 10−1 s−1) surpasses the 325°C-forged state (750 % at 5.6×10−3 s−1). This is attributed to enhanced dislocation density accelerating diffusion and dynamic recrystallization; however, at >450°C, the same feature causes abnormal grain growth, revealing the dual role of pre-stored defects in superplasticity. Comparison with subsequent rolling data showed that two-step MF provides a gain in sheet strength (up to 540 MPa) but significantly suppresses superplasticity. Thus, forging at 250°C may be considered a critical regime; further temperature decrease could risk structural instability and embrittlement. This route is recommended for bulk products or high-strength sheets when high-temperature processing is not required.

Ссылки (44)

3. R. R. Mulyukov, R. M. Imayev, A. A. Nazarov, et al, Superplasticity of ultrafine grained alloys: Experiment, theory, technologies, Nauka, Moscow, 2014. (in Russian) [Р. Р. Мулюков, Р. М. Имаев, А. А. Назаров, и др., Сверхпластичность ультрамелкозернистых сплавов: эксперимент, теория, технологии, Наука, Москва, 2014.].
8. O. R Valiahmetov, R. M Galeyev, G. A Salishchev, Mechanical properties of VT 8 Ti-alloy of submicrocrystalline structure. Fiz. Met. Metallog, 10 (1990) 204 - 206. (in Russian) [О. Р. Валиахметов, Р. М. Галеев, Г. А. Салищев, Механические свойства титанового сплава ВТ8 с субмикрокристаллической структурой, Физика металлов и металлография 10 (1990) 204 - 206.].
10. V. V. Zakharov, Effect of scandium on the structure and properties of aluminum alloys, Met. Sci. and H. Treat. 45 (2003) 246 - 253.
11. E. Avtokratova, O. Sitdikov, O. Mukhametdinova, M. Markushev, S. V. S. N. Murty, M. J. N. V. Prasad, B. P. Kashyap, Microstructural evolution in Al-Mg-Sc-Zr alloy during severe plastic deformation and annealing, J. All. Comp. 673 (2016) 182 -194.
17. О. Sh. Sitdikov, Е. V. Avtokratova, О. E. Мukhametdinova, R. N. Garipova, R. R. Ilyasov, М. V. Мarkushev, Microstructure, mechanical properties and thermal stability of the ultrafine grained Al-Mg-Sc-Zr alloy processed by multy-directional isothermal forging, Mater. Phys. Mech. 33 (1) (2017) 137 -151. (in Russian) [О. Ш. Ситдиков, Е. В. Автократова, О. Э. Мухаметдинова, Р. Н. Гарипова, Р. Р. Ильясов, М. В. Маркушев, Микроструктура, механические свойства и термическая стабильность ультрамелкозернистого Al-Mg-Sc-Zr сплава, полученного всесторонней изотермической ковкой, Механика и физика материалов, 33 (1) (2017) 137 -151.]
21. F. J. Humphreys and M. Hatherly, PAST II: Recrystallization and Related Annealing Phenomena, Elsevier, Amsterdam, 2004, 658 p.
27. M. E. Kassner, M. T. Perez-Prado, Fundamentals of Creep in Metals and Alloys, Elsevier, Netherlands, 2004, 272 p.
29. J. Čadek, Creep in Metallic Materials, Elsevier, New York, 1988, 372 p.
30. A. Bhaduri, Mechanical properties and working of metals and alloys, Springer Series in Materials Science, 264 (2018) 748.

Финансирование на английском языке

1. The work was carried out under the state assignment of IMSP RAS. Experimental studies were performed using the facilities of shared services center of IMSP RAS -