Аннотация

Grain-oriented electrical steel (GOES) is characterized by a strong crystallographic texture, which is crucial for its magnetic properties. However, this texture also induces significant anisotropy in its elastic characteristics, which is less studied but important for manufacturing and application. This work investigates the anisotropy of the elastic modulus in GOES at different stages of its production — specifically after the first cold rolling (CR1), after subsequent decarburization−recrystallization annealing (DRA), and after the second cold rolling (CR2). The study employs a combined approach using Electron Backscatter Diffraction (EBSD) for texture analysis and Dynamic Mechanical Analysis (DMA) for direct measurement of storage modulus. Using the EBSD analysis the evolution of the crystallographic texture across the manufacturing stages was studied. The key texture components were qualified and quantified by 20° deviation of standard crystallographic directions <100>, <110> and <111> from CR axes: RD, TD and ND. These data were compared to the spatial maps of Young’s modulus, showing a uniform distribution in the rolling direction (RD) and the greatest dispersion of values in the normal direction (ND) for all processing stages. The maximum modulus values were consistently observed in the transverse direction (TD). A comparative analysis demonstrated a correlation between the elastic moduli values obtained via EBSD calculations and direct DMA measurements. A more significant divergence was noted for the thinner CR2 sheet (0.27 mm), which is attributed to the specific stress state during three-point bending in DMA, which amplifies the contribution of the near-surface layers.
Ссылки (29)
1.
A. A. Redikultsev, M. L. Lobanov, M. A. Zorina, D. D. Satskii, Mechanism of structural-textural heredity in grain oriented electrical steel. 1. Secondary recrystallization, Metal Science and Heat Treatment, 3 (2025) 3 - 9. (in Russian) [А. А. Редикульцев, М. Л. Лобанов, М. А. Зорина, Д. Д. Сацкий, Механизм структурно-текстурной наследственности в электротехнической анизотропной стали. 1. Вторичная рекристаллизация, Металловедение и Термическая Обработка Металлов 3 (2025) 3 - 9.]2.
A. A. Redikultsev, M. L. Lobanov, M. A. Zorina, D. D. Satskii, Mechanism of structural-textural heredity in grain oriented electrical steel. 2. Evolution of the main crystallographic orientations, Metal Science and Heat Treatment, 3 (2025) 10 -17. (in Russian) [А. А. Редикульцев, М. Л. Лобанов, М. А. Зорина, Д. Д. Сацкий, Механизм структурно-текстурной наследственности в электротехнической анизотропной стали. 2. Эволюция основных кристаллографических ориентировок, Металловедение и Термическая Обработка Металлов (2025) 10 - 17.]4. T. Kumano, T. Haratani, Y. Ushigami, The Relationship between Primary and Secondary Recrystallization Texture of Grain Oriented Silicon Steel, ISIJ International 42 (2002) 440 - 449.
8. M. L. Lobanov, A. A. Redikultsev, M. A. Zorina, Metalphysics of materials for electromechanical engineering, Ekaterinburg Ural University Publisher House, 144 p. (in Russian) [М. Л. Лобанов, А. А. Редикульцев, М. А. Зорина, Металлофизика материалов для электромашиностроения Учебное пособие, Издательство Уральского университета, Екатеринбург, 2019, 144.].
11. Y. N. Loginov, M. P. Puzanov, Influence of properties anisotropy on stress-deformed state at rolling of stripes from electrical STEEL, Chernye Metally 1042 (2018) 22 - 27. (in Russian) [Ю. Н. Логинов, М. П. Пузанов, Влияние анизотропии свойств на напряженнодеформированное состояние при прокатке полосы из электротехнической стали, Черные металлы 1042 (2018) 22 - 27.].
12.
F. Gao, Y. Chen, Q. Zhu, Y. Nan, S. Tang, Z. Cai, F. Zhang, W. Xue, X. Cai, F. Yu, Z. Liu, Formation of recrystallization texture and its effect on deep drawability for high-purified ferritic stainless steel by two step cold rolling, Mater. Des. 226 (2023) 11167913.
F. Gao, Q. Zhu, W. Xue, Y. Chen, F. Zhang, Y. Nan, S. Tang, J. Zhang, D. Tie, X. Cai, F. Yu, Z. Liu, Correlation between formability, ridging and recrystallization texture development in ferritic stainless steel fabricated by introducing intermediate annealing during cold rolling, Mater. Charact. 205 (2023) 11329619. F.J. Humphreys, M. Hatherly, Recrystallization and related annealing phenomena second edition, 2nd ed., Elsevier Ltd., Oxford, 2004.
22. S. Satyam, David P. Field, Advances in Texture, Microtexture, and Allied Techniques, 1st ed., Materials Horizons: From Nature to Nanomaterials, 2025.
24.
A. A. Redikul’tsev, M. A. Zorina, V. I. Pastukhov, M. L. Lobanov, The role of special boundaries in structural and phase transformations in metals and alloys. 1. Deformation and recrystallization, Metal Science and Heat Treatment 9 (2025) 6 -11. (in Russian) [А. А. Редикульцев, М. А. Зорина, В. И. Пастухов, М. Л. Лобанов, Роль специальных границ при структурных и фазовых превращениях в металлах и сплавах. 1. Деформация и рекристаллизация, Металловедение и термическая обработка металлов 9 (2025) 6 -11.]25.
A. A. Redikul’tsev, M. A. Zorina, V. I. Pastukhov, M. L. Lobanov, The role of special boundaries in structural and phase transformations in metals and alloys. 2. Phase transformations, Metal Science and Heat Treatment 9 (2025) 12 -18. (in Russian) [А. А. Редикульцев, М. А. Зорина, В. И. Пастухов, М. Л. Лобанов, Роль специальных границ при структурных и фазовых превращениях в металлах и сплавах. 2. Фазовые превращения, Металловедение и термическая обработка металлов 9 (2025) 12 -18.]
Финансирование на английском языке
1. Russian Science Foundation - 25-19-00683